乙酰苯胺的制备(2)

2021-01-20 22:26

料中间体对硝基乙酰苯胺、对硝基苯胺和对苯二胺。在工业上可作橡胶硫化促进剂、纤维脂涂料的稳定剂、过氧化氢的稳定剂,以及用于合成樟脑等。 用冰醋酸做乙酰化试剂与苯胺制备乙酰苯胺,三组取不同量的试剂分别制备乙酰苯胺。用热水进行重结晶,精制乙酰苯胺,称重计算产率。分析乙酸苯胺制备过程中应注意的事项,以及影响产率的因素。

关键词:乙酰苯胺 制备 重结晶

Abstract

Abstract: sulfa drugs acetanilide is the raw material, can be used as analgesics, antipyretic agents and preservatives. Used to make dyes intermediates of nitro acetanilide, p-nitroaniline and p-phenylenediamine. In the industrial rubber vulcanization accelerator can be used for fiber coating resin stabilizer, hydrogen peroxide stabilizer, as well as for synthetic camphor and so on.

To do with glacial acetic acid and aniline acetylation reagent preparation acetanilide, three take different amounts of reagents were prepared acetanilide. Recrystallized with hot water, refined acetanilide, weighing calculate yield. During the preparation of acetic acid Aniline precautions, as well as the factors that affect yield.

Key words:sulfa drugs acetanilide, preparation ,recrystallization


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