(4)塔顶温度tD下的汽化潜热
内插法计算出塔顶温度下的汽化潜热。 乙醇的汽化潜热:
?乙醇,-?乙醇,?-?乙醇,820.5-810.180℃70℃80℃79.80℃?乙醇,?80-7080-79.8080-70
820.5-?乙醇,79.80℃?80-79.80??乙醇,-?820.3kj?kg-1 79.80℃正丙醇的气化潜热:
?正丙醇,-?正丙醇,?-?正丙醇,690.5-673.380℃70℃80℃79.80℃?正丙醇,?80-7080-79.8080-70 690.5-?正丙醇,79.80℃?80-79.80??正丙醇,-?689.2kj?kg-1 79.80℃??D?xD?乙醇,79.80?(1?xD)?正丙醇,79.80?0.9215?820.3?(1-0.9215)?689.2?810.0kJ?kg-12.3.4.热量衡算
(1)0℃时塔顶上升的热量Qv 塔顶以0℃为基准
QV?VCPDtD?V?DMVD
?192.02?162.64?79.80?192.02?810.0?47.17?9828807.2kJ?h-1
(2)回流液的热量QR
根据t-x-y图查得此时组成下的泡点tD=79.20℃
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此温度下,
Cp乙醇,80℃-Cp乙醇,70℃?80-703.48-Cp乙醇,79.20℃80-79.203.48-3.25Cp乙醇,80℃-Cp乙醇,79.20℃??80-7080-79.20
?Cp乙醇,79.20℃?3.462kJ/(kg?K)
正丙醇的比热容:
Cp正丙醇,80℃-Cp乙醇,70℃?80-703.13-Cp乙醇,79.20℃80-79.20?3.13-3.00Cp正丙醇,80℃-Cp正丙醇,79.20℃?80-7080-79.20
?Cp正丙醇,79.20℃?3.120kJ/(kg?K)
?CpR?xRCp乙醇,79.20℃?(1?xR)CP正丙醇,79.20℃
?0.9215?3.462?(1-0.9215)?3.120?3.435kJ/(kg?K)
?162.03kJ/(kmol?K)QR?LCpRtR?143.35?162.03?78.20?1816351.439kJ?h-1
(3)塔顶馏出液的热量QD
因馏出口与回流口组成相同,所以
CpD?162.64kJ/(kmol?K)
QD?DCpDtD?28.67?162.64?79.80?372098.53kJ?h-1 (4)进料的热量QF
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QF?FCpFtF?64.04?183.86?87.21?1026844.941kJ?h-1
(5)塔底残液的热量QW
QW?WCpWtW?35.37?199.26?97.60?687867.84kJ?h-1 (6)冷凝器消耗的热量QC
QC?QV?QR?QD?9828807.2?1816351.439-372098.53?7640357.2 kJ?h-1(7)再沸器提供热量QB(全塔范围列热量衡算式)
取塔釜热量损失为10%,则Q损?0.1QB,
QB?QF?QC?QW?QD?Q损
再沸器的实际热负荷:
0.9QB?QC?QW?QD-QF ?7640357.2?687867.84?372098.53-1026844.94
?7673478.63kJ?h-1计算得:QB?8526087.37kJ?h-1 计算结果见下表:
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热量衡算计算结果
项目 平均比热容/[kJ/(kmol?K)]
进料 冷凝器
塔顶流出
液 162.64
塔底流出
液 199.26
再沸器
183.86 1026844.94
—— 7640357.2
—— 8526087.4
热量Q/(kJ?h-1)
372098.53 687867.84
2.4 塔径的初步计算
(1)精馏段
由u=(安全系数)* umax,安全系数=0.6-0.8, umax?c?1??L??V ?V?Ls1?L1?9.91739.100.5?2?横坐标数值:?()??()?0.042
Vs1?V14876.221.73取板间距:Ht=0.45m , hL=0.07m .则Ht- hL=0.38m
?17.670.2查图可知C20=0.082 , c?c20()?0.082?()?0.080
2020umax?0.08
u1?0.7umaxD1?739.10?1.73?1.652m/s1.73?0.7?1.652?1.156m/s4Vs14?4876.22??1.493m?u13.14?1.156?3600
圆整:D1?1.6mAT?0.785?1.62?2.01m2横截面积:
??空塔气速:u1 4876.22?0.67m/s3600?2.01(2)提馏段
1Ls2?L2116.13736.57横坐标数值:?()2??()2?0063
Vs2?V24993.981.91 22
取板间距:Ht=0.45m , hL=0.07m .则Ht- hL=0.38m
?17.550.2查图可知C20=0.082 , c?c20()?0.082?()?0.080
2020736.57?1.91?1.569m/s1.91??0.7umax?0.7?1.569?1.098m/su2?ax?0.080?umD2?4Vs2???u24?4993.98?1.28m;3.14?1.098?3600
圆整:D2?1.6m横截面积
AT?0.785?1.62?2.01m2??空塔气速:u2
4993.98?0.69m/s2.01?36002.5 溢流装置
lW2.5.1堰长
取lw?0.7D?0.7?1.6?1.12m 溢流堰高度hW hW?hL?hOW 选择平直堰
堰上层高度hOW?(1)精馏段
2.84?E(Lh/lW)2/31000
22.849.913how??()?0.012m 10001.12hw?hL?how?0.07?0.012?0.058m 23