MVF,m?0.930?78.11??1?0.930??112.61?80.52kg/kmol MLD,m?0.728?78.11??1?0.728??112.61?87.49kg/kmol
精馏段:MV,m??78.59?80.52?/2?79.56kg/kmol
ML,m??80.18?87.49?/2?83.84kg/kmol
4.平均密度ρm 1)液相平均密度ρL,m
塔顶:?LD,A?912.13?1.1886t?912.13?1.1886?80.5?816.4kg/m3
?LD,B?1124.4?1.0657t?1124.4?1.0657?80.5?1038.6kg/m3
1?LD,m?aA?LD,A?aB?LD,B?0.980.02???LD,m?819.9kg/m3 816.41038.6进料板:ρLF,A?912.13?1.1886t?912.13?1.1886?88?807.5kg/m3
ρLF,B?1124.4?1.0657t?1124.4?1.0657?88?1030.6kg/m3 1ρLF,m?aAa0.650.35?B???ρLF,m?873.7kg/m3 ρLF,AρLF,B807.51030.63精馏段:?L,m??819.9?873.7?/2?846.8kg/m 2)汽相平均密度ρV,m
?V,m?pmMV,mRTm?108.1?79.56?2.896kg/m3
8.314??273?84.2?5.液体的平均表面张力σm
塔顶:?D,A?21.1mN/m;?D,B?25.9mN/m(80.5℃)
?D,m?????A?B21.1?25.9???????21.15mN/m
?x??x21.1?0.014?25.9?0.986???ABBA?D进料板:σF,A?20.20mN/m;σF,B?25.34mN/m(88℃)
?σAσBσF,m???σx?σxBA?AB?20.20?25.34???????21.38mN/m ?20.20?0.272?25.34?0.728??F?- 11 -
精馏段:?m??21.15?21.38?/2?21.26mN/m 6.液体的平均粘度μL,m
塔顶:查化工原理附录,在80.5℃下有:
μLD,m??μAxA?D??μBxB?D?0.315?0.986?0.445?0.014?0.317mPa?s
加料板:在88℃下有:?LF,m?0.28?0.728?0.41?0.272?0.315mPa?s 精馏段:μL,m??0.317?0.315?/2?0.316mPa?s (五)精馏段的汽液负荷计算
汽相摩尔流率V??R?1?D?1.499?159.40?238.94kmol/h 汽相体积流量Vs?VMV,m3600?V,m?238.94?79.56?1.823m3/s
3600?2.896汽相体积流量Vh?1.823m3/s?6563m3/h
液相回流摩尔流率L?RD?0.499?159.40?79.54kmol/h 液相体积流量Ls?LML,m3600?L,m?79.54?83.84?0.00219m3/s
3600?846.8液相体积流量Lh?0.00219m3/s?7.884m3/h
冷凝器的热负荷Q?Vr??238.94?78.59??310?/3600?1617kW (六)塔和塔板主要工艺结构尺寸的计算 1.塔径
1)初选塔板间距HT?500mm及板上液层高度hL?60mm,则:
HT?hL?0.5?0.06?0.44m
2)按Smith法求取允许的空塔气速umax(即泛点气速uF)
?Ls???L?????V??s??V?0.5?0.00219??846.8???????1.823??2.896?0.5?0.0205
查Smith通用关联图得C20?0.0935
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负荷因子C?C20?泛点气速:
?????20?0.2?21.26??0.0935???20?0.2?0.0946
umax?C3)操作气速
??L??V?/?V?0.0946?846.8?2.896?/2.896?1.615m/s
取u?0.7umax?1.13m/s 4)精馏段的塔径
D?4Vs/?u?4?1.823/3.14?1.13?1.433m
圆整取D?1600mm,此时的操作气速u?0.907m/s。 2.塔板工艺结构尺寸的设计与计算 1)溢流装置
采用单溢流型的平顶弓形溢流堰、弓形降液管、平形受液盘,且不设进口内堰。 ①溢流堰长(出口堰长)lw
取lw?0.7D?0.7?1.6?1.12m
堰上溢流强度Lh/lw?7.884/1.12?7.039m/?m?h??100~130m/?m?h?,满足筛
33板塔的堰上溢流强度要求。 ②出口堰高hw
hw?hL?how
对平直堰how?0.00284E?Lh/lw?2.52/3
2.5由lw/D?0.7及Lh/lw?7.884/1.12 ?5.939,查化工原理图得E?1.07,于是:
how?0.00284?1.07?7.884/1.12?2/3?0.01116m?0.006m(满足要求)
hw?hL?how?0.06?0.01116?0.0488m
③降液管的宽度Wd和降液管的面积Af
由lw/D?0.7,查化原下P147图11-16得Wd/D?0.14,Af/AT?0.09,即:
Wd?0.224m,AT?0.785D2?2.01m2,Af?0.181m2。
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液体在降液管内的停留时间
??AfHT/Ls?0.181?0.5/0.00219?41.32s?5s(满足要求)
④降液管的底隙高度ho
液体通过降液管底隙的流速一般为0.07~0.25m/s,取液体通过降液管底隙的流速
??0.08m/s,则有: uoho?Ls0.00219??0.0244m(ho不宜小于0.02~0.025m,本结果满足要求) ?1.12?0.08lwuo2)塔板布置
①边缘区宽度Wc与安定区宽度Ws
边缘区宽度Wc:一般为50~75mm,D >2m时,Wc可达100mm。
安定区宽度Ws:规定D?1.5m时Ws?75mm;D?1.5m时Ws?100mm; 本设计取Wc?60mm,Ws?100mm ②开孔区面积Aa
π2x??Aa?2?xR2?x2?Rsin?1?180R??π0.476?? ?2?0.4760.742?0.4762??0.742sin?1?1800.740???1.304m2式中:x?D/2??Wd?Ws??0.8??0.224?0.100??0.476m
R?D/2?Wc?0.8?0.060?0.740m
3)开孔数n和开孔率υ
取筛孔的孔径do?5mm,正三角形排列,筛板采用碳钢,其厚度δ?3mm,且取
t/do?3.0。故孔心距t?3?5?15mm。
?1158?103??1158?103???Aa???1.304?6711(孔) 每层塔板的开孔数n??22????t???15?每层塔板的开孔率υ?0.907?t/do?2?0.907?0.101(υ应在5~15%,故满足要求) 23- 14 -
每层塔板的开孔面积Ao?υAa?0.101?1.304?0.132m2 气体通过筛孔的孔速uo?Vs/Ao?1.823/0.132?13.81m/s 4)精馏段的塔高Z1
Z1??Np1?1?HT??8?1??0.5?3.5m
(七)塔板上的流体力学验算 1.气体通过筛板压降hp和Δpp的验算
hp?hc?hl?hσ
1)气体通过干板的压降hc
?u???13.81?2.896hc?0.051?o?V?0.051??0.0520m ??0.8?846.8?Co??L式中孔流系数Co由do/δ?5/3?1.67查图得出,Co?0.8。 2)气体通过板上液层的压降hl
22hl?β?hw?how??βhL?0.6?0.06?0.036m
式中充气系数β的求取如下:
气体通过有效流通截面积的气速ua,对单流型塔板有:
ua?Vs1.823??0.997m/s
AT?Af2.01?0.181动能因子Fa?ua?V?0.9972.896?1.697
查化原图得β?0.60(一般可近似取β?0.5~0.6)。 3)气体克服液体表面张力产生的压降hσ
4?4?21.26?10?3h????0.00205m
?Lgdo846.8?9.81?0.0054)气体通过筛板的压降(单板压降)hp和Δpp
hp?hc?hl?h??0.0520?0.036?0.00205?0.090m
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