数 据 处 理 系 统
PDA-WIN
操作手册
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岛津公司
目 录
第一章 工作原理................................................................................................................1-2 1.1 工作曲线...........................................................................................................1-2 1.2 再标准化..................................……………………………………………….1-3 1.3 共存元素修正...................................................................................................1-5 1.4 100%修正..........................................................................................................1-8 1.5 主曲线修正(控样修正)...............................................................................1-10 1.6 近似含量分析...................................................................................................1-12
第二章 仪器的准备
2.1 计算机的设置....................................................................................................2-2 ⑴ 安装SCSI接口...............................................................................................…2-2 ⑵ 联结 CPU 控制装置......................................................................................2-3 ⑶ 安装SCSI接口软件...........................................................................................2-4
2.2 Windows基本操作过程..................................................................…................2-5
⑴ 鼠标的操作................................................................................................….........2-5 ⑵ 窗口的操作.................................................................................................…........2-6
2.3 基本操过程
2.4 PDA-WIN 的结构.....................................................................................……2-14
2.5 仪器的启动与停止.........................................................................................….2-17 ⑴ 仪器的启动...........................................................................................................2-17 ⑵ 仪器的停止.......................................................................................................…..2-18
第三章 准备
3.1 耗费放电....................................................................……………………………3-2 3.2 手动扫描................................................................................................................3-4 3.3 调整灵敏度............................................................................................................3-8 3.4 再标准化目标值的测量...................................................................................….3-10 3.5 工作曲线用测量.................................................................................................…3-12
第四章 建立工作曲线.................................................................................................... ….4-2
4.1 工作曲线/共存元素修正系数的计算....................................................................4-2
⑴ 工作曲线/共存元素修正系数的计算.....................................................................4-2
⑵ 设定共存元素.....................................................................................................….4-5
⑶ 数据窗口...............................................................................................................4-6 ⑷ 数据表窗口...........................................................................................................4-7 ⑸ 工作曲线的分割...................................................................................................4-8 ⑹ 工作曲线的使用范围...........................................................................................4-8 ⑺ 建立工作曲线用样品的登记...............................................................................4-9 ⑻ 曲线图的放大输入/输出.............................................................................…......4-10 ⑼ 任选设定...........................................................................................................…4-11
第五章 含量分析
5.1 含量分析用准备...........................................................................................................5-2 5.2 含量分析...................................................................................................................…5-3 5.3 含量分析的基本操作...................................................................................................5-4 ⑴ 分析结果的显示............................................................................................................5-4 ⑵ 按钮功能........................................................................................................................5-5 ⑶ 分析组的选择................................................................................................................5-6 ⑷ 辅助分析........................................................................................................................5-7 ⑸ 分析的取消....................................................................................................................5-7 ⑹ 分析的结束....................................................................................................................5-7 ⑺ 恢复分析........................................................................................................................5-7 ⑻ 分析方式........................................................................................................................5-8 ⑼ 频率分布........................................................................................................................5-11 ⑽ 时序轮廓........................................................................................................................5-12 ⑾ 打印设定........................................................................................................................5-13 ⑿ 激发次数的数的控制...................................................................................................5-15
5.4 再标准化分析..............................................................................................................5-16
5.5 控样修正分析..............................................................................................................5-19
5.6 含量分析......................................................................................................................5-22 ⑴ 什么是含量分析...........................................................................................................5-22 ⑵ 含量分析(多次分析)................................................................................................5-23
5.7 含量分析的应用...........................................................................................................5-25 ⑴ 含量分析(4次分析).................................................................................................5-25 ⑵ 近似含量分析...............................................................................................................5-28 ⑶ 粗略分析.......................................................................................................................5-29 ⑷ 含量分析时合金判定...................................................................................................5-31
第六章 设定情报
6.1 系统情报......................................................................................................................6-2
⑴ 分析组的构成...............................................................................................................6-4 ⑵ 分析情报的基本操作过程...........................................................................................6-5
6.2 分析条件情报...............................................................….............................................6-6 ⑴ 分析情报窗口...............................................................................................................6-6 ⑵ 分析组的详细设定.......................................................................................................6-8 ⑶ 分析条件..................................................................................................................….6-10 (3-1)分析条件..................................................................................................................6-10 (3-2)测量条件的详细设定..............................................................................................6-13 ⑷ 灵敏度情报...................................................................................................................6-17 ⑸ 分析元素...................................................................................................................... 6-18 ⑹ 分析通道情报...............................................................................................................6-20 ⑺ 测量方式.................................................................................................................…..6-22 ⑻ 再标准化情报...........................................................................................................…6-25
6.3 工作曲线情报........................………………………………………………………6-27 ⑴ 工作曲线和共存元素修正系数.................................................................................6-28 ⑵ 100%修正情报............................................................................................................6-29
6.4 分析组情报................................................................................................................6-30 ⑴ 标准情报.....................................................................................................................6-30 ⑵ 显示和打印/传输情报............................................................................................…6-31 ⑶ 空样修正分析情报.....................................................................................................6-33 ⑷ 分析方式情报.............................................................................................................6-35 ⑸ 质量评估图情报.........................................................................................................6-39
6.5 其它情报....................................................................................................................6-41 ⑴ 近似含量分析情报.....................................................................................................6-41 (1-1)近似分析条件........................................................................................................6-41 (1-2)近似分析评定条件的登记....................................................................................6-43 ⑵ R控制情报..................................................................................................................6-44 ⑶ 特殊计算式情报..........................................................................................................6-46 ⑷ 合金搜索......................................................................................................................6-48 (4-1)合金搜索组的登记.............................................................................................…6-48 (4-2)合金规格的登记.....................................................................................................6-50 (4-3)合金规格的范围登记.............................................................................................6-52 ⑸ 分析程序......................................................................................................................6-53 ⑹ 分析范围情报..............................................................................................................6-55 ⑺ 化学分析值的登记......................................................................................................6-57
第七章 结果管理
7.1 基本操作.................................................................................................................7-2 ⑴ 什么是结果管理?..................................................................................................7-2 ⑵ 主窗口......................................................................................................................7-3 ⑶ 数据搜索..................................................................................................................7-5 ⑷ 选择数据..................................................................................................................7-7 ⑸ 选择数据库..............................................................................................................7-8
7.2 质量评估图.............................................................................................................7-9 ⑴ 质量评估图................................................................................................................7-9 ⑵ 设定扫质量评估图描线..........................................................................................7-10 ⑶ 质量评估图的分析值数据表..................................................................................7-11 ⑷ 质量评估图分析数据窗口......................................................................................7-11
7.3 直方图.......................................................................................................................7-12 ⑴ 直方图......................................................................................................................7-12 ⑵ 设定直方图的扫描线情报......................................................................................7-12 7.4 日 报.................................................................................................................7-14 7.5 查阅数据.................................................................................................................7-15 7.6 删除数据.................................................................................................................7-17 7.7 数据转换.....................……………………………………………………………7-17 7.8 拷贝数据...............................................................................................….............7-18 7.9 新增数据(计算平均值)..................................................................…..............7-18 7.10 选择设定数据管理............................................................................…..............7-19
第八章 S/W的其它功能..................................................................................…...............8-2
8.1 仪器检查.............................................................................................…...............8-2 8.2 修正前强度分析.................................................................................…...............8-5 8.3 测量漂移修正后强度........................................................................…................8-7 8.4 灯试验.................................................................................................…...............8-9 8.5 资料保存..............................................................................................…..............8-12
⑴ 建立备份................................................................................................….............8-14 ⑵ 备份的恢复.............................................................................................…............8-16 ⑶ ADS备份文件的转换.........................................................................…...............8-17
8.6 系统的安装.........................................................................................…...............8-19 8.7 口 令............................................................................................…................8-22 8.8 帮 助............................................................................................…................8-23 8.9 版 本.............................................................................................…...............8-24