MilkoScan FT-120乳品分析仪
操作手册
Foss China Application Team
2004年3月
目录
MilkoScan FT 120乳品分析仪操作手册
第1章 简介 ............................................................................................................................................ 6 §1. 1 FT—120乳品分析仪 ................................................................................................................. 6 §1. 2 关于这本手册 ............................................................................................................................ 6 §1. 3 福斯电子的定标模块 ................................................................................................................ 7 §1. 4 FT—120 仪器可选模块 .......................................................................................................... 7 §1. 4. 1自动清洗和调零模块(ACZ) .............................................................................................. 7 §1. 4. 2 应用模块 ........................................................................................................................... 7 §1. 4. 3 天平选项 ........................................................................................................................... 7 §1. 4. 4 高级性能模块 ................................................................................................................... 8 §1. 4. 5高级定标使用模块............................................................................................................. 8 §1. 4. 6 输入选项 ........................................................................................................................... 8 §1. 4. 7 数据交换选择模块（DDE） ........................................................................................... 8 §1. 4.8 质量保证模块 .................................................................................................................... 8 §1. 5 WINDOWS系统 ............................................................................................................................ 9 §1. 5. 1 菜单栏 ............................................................................................................................... 9 §1. 5. 2 功能键 ............................................................................................................................... 9 §1. 5. 3 按钮栏 ............................................................................................................................... 9 §1. 5. 4 滚动栏 ............................................................................................................................. 10 §1. 5. 5 状态栏 ............................................................................................................................. 10 §1. 6 定义自己的窗口 ...................................................................................................................... 10 §1. 7 仪器语言支持 .......................................................................................................................... 11 §1. 7. 1 怎样使用当地语言 .......................................................................................................... 11 §1. 8 激光的保险装置 ...................................................................................................................... 11 第2章 FT—120乳品分析仪用户界面 .............................................................................................. 12 §2. 1 FT—120乳品分析仪插图屏幕说明 ........................................................................................ 12 §2. 2 按钮板 ...................................................................................................................................... 13 §2. 3 功能键 ...................................................................................................................................... 13 §2. 4 快捷键 ...................................................................................................................................... 14 §2. 5 其它菜单 .................................................................................................................................. 14 §2. 6 菜单概要 .................................................................................................................................. 15 §2.6.1 菜单中的基本模块............................................................................................................ 15 §2.6.2 应用模块中的菜单............................................................................................................ 16 §2. 7 物理连接与转换 .......................................................................................................................... 第3章 操作 .......................................................................................................................................... 18 §3. 1 调零和稳定性样品 .................................................................................................................. 18 §3. 1. 1 开机 ................................................................................................................................. 18 §3. 1. 2 清洗仪器 ......................................................................................................................... 18 §3. 1. 3 调零 ................................................................................................................................. 18 §3. 1. 4 使用稳定性样品对仪器检测 .......................................................................................... 18 §3. 2 仪器标准化 .............................................................................................................................. 19 §3. 3 样品的测量 .............................................................................................................................. 19 §3. 3. 1 样品 ................................................................................................................................. 19 §3. 3. 2 样品保存 ......................................................................................................................... 19 福斯中国应用技术部 2 Foss China Application Team
MilkoScan FT 120乳品分析仪操作手册
§3. 3. 3 贮存 ................................................................................................................................. 19 §3. 3. 4 预热 ................................................................................................................................. 19 §3. 3. 5 清洗与除气 ..................................................................................................................... 20 §3. 3. 7 产品的选择 ..................................................................................................................... 20 §3. 3. 8 样品编号和注解的输入 .................................................................................................. 21 §3. 3. 9 稀释样品 ......................................................................................................................... 21 §3. 3. 10 定标样品 ....................................................................................................................... 21 §3. 3. 11 开始分析 ........................................................................................................................ 21 §3. 3. 12 测试的中断 ................................................................................................................... 23 §3.4 关机 ........................................................................................................................................... 23 §3. 5 清洗程序 .................................................................................................................................. 23 §3. 5. 1 清洁剂彻底清洗.............................................................................................................. 23 §3. 5. 2 强力清洗 ......................................................................................................................... 23 §3. 5. 3次氯酸盐 .......................................................................................................................... 24 §3. 6 自动清洗和调零 ...................................................................................................................... 24 第4章 分析稀释的样品 ...................................................................................................................... 26 4.1做稀释样品.................................................................................................................................. 26 4.2稀释系列样品 .............................................................................................................................. 26 4.3稀释程序...................................................................................................................................... 28 4.4运用天平选项的稀释 .................................................................................................................. 29 4.5人工输入稀释数据 ...................................................................................................................... 32 4.6 在分析前检查和改变稀释 ......................................................................................................... 32 4.7分析前取消稀释 .......................................................................................................................... 33 4.8分析后检查稀释率 ...................................................................................................................... 33 第5章 结果的处理 .............................................................................................................................. 34 §5. 1 追踪模式 .................................................................................................................................. 34 §5. 2 结果编辑 .................................................................................................................................. 35 第6章 打印和结果输出 ...................................................................................................................... 36 §6. 1 打印结果文件 .......................................................................................................................... 36 §6. 2 打印产品说明 .......................................................................................................................... 36 §6. 3 输出结果文件 .......................................................................................................................... 38 §6. 4 定义输出“过滤器” .............................................................................................................. 39 §6. 5 输出和输入产品程序 .............................................................................................................. 40 第7章 设备工作原理 .......................................................................................................................... 41 §7.1 流路系统 ................................................................................................................................... 41 §7.2 流路系统工作原理 ................................................................................................................... 42 §7.3傅立叶变换红外测试原理 ........................................................................................................ 42 §7. 3. 1 干涉仪的基本原理 .......................................................................................................... 42 §7. 3. 2 傅立叶变换原理.............................................................................................................. 43 第8章 软件设置和维护 ...................................................................................................................... 44 §8. 1 启动程序 .................................................................................................................................. 44 福斯中国应用技术部 3 Foss China Application Team
MilkoScan FT 120乳品分析仪操作手册
§8. 1. 1 观察系统信息 ................................................................................................................. 45 §8. 2 设定FT－120乳品分析仪系统软件 ...................................................................................... 45 §8. 2. 1 综合参考 ......................................................................................................................... 45 §8. 2. 2 分析设置 ......................................................................................................................... 46 §8. 2. 3 警告设置 ......................................................................................................................... 47 §8. 2. 4使用自动清洗和调零模块分析时设置 ........................................................................... 47 §8. 2. 5 使用天平选项进行稀释设定 .......................................................................................... 48 §8. 2. 6 设定时间和日期.............................................................................................................. 49 §8. 2. 7 密码设置 ......................................................................................................................... 50 §8. 3 数据库的安全 .......................................................................................................................... 50 §8. 3. 1 数据库的保险装置级别选择 .......................................................................................... 50 §8. 3. 2 使用一个U P S ............................................................................................................... 50 §8.4 数据库的维护 ........................................................................................................................... 52 §8. 4. 1 启动数据库维修程序 ...................................................................................................... 52 §8. 4. 2 自动清除和备份.............................................................................................................. 53 §8. 5 备份 .......................................................................................................................................... 53 §8. 5. 1 恢复备份数据 ................................................................................................................. 53 §8. 6 FT－120乳品分析仪软件的许可证 ........................................................................................ 54 §8. 6. 1 软钥匙系统 ..................................................................................................................... 54 第9章 仪器维修 .................................................................................................................................. 55 §9. 1 仪器检查 .................................................................................................................................. 55 §9. 1. 1 清洗 ................................................................................................................................. 55 §9. 1. 2 零点稳定性 ..................................................................................................................... 56 §9. 1. 3 稳定性（样品）检查 ...................................................................................................... 56 §9．1．4 均质器检查 ................................................................................................................. 58 §9．1．5 清洗效率检查.............................................................................................................. 58 §9．1．6 吸入量检查 ................................................................................................................. 59 §9．1．7 定标检查 ..................................................................................................................... 59 §9．1．8 重现性检查 ................................................................................................................. 59 §9．1．9 温度稳定性检查 .......................................................................................................... 60 §9．1．10 FTIR平衡标准化 .................................................................................................... 60 §9．1．11 线性化检查 ................................................................................................................ 61 §9．2 维修 ........................................................................................................................................ 61 §9．2．1 吸管过滤器 ................................................................................................................. 62 §9．2．2 蠕动泵 ......................................................................................................................... 62 §9．2．3 热交换器 ..................................................................................................................... 63 §9．2．4 单向阀 ......................................................................................................................... 64 §9．2．5 截止阀 ......................................................................................................................... 65 §9．2．6 均质塞 ......................................................................................................................... 65 §9．2．7 背压阀 ......................................................................................................................... 66 §9．2．8 在线过滤器 ................................................................................................................. 67 §9．2．9 观察室 ......................................................................................................................... 68 §9．2．10 样品架 ....................................................................................................................... 69 §9．2．11 废液桶感应器 ............................................................................................................ 70 福斯中国应用技术部 4 Foss China Application Team
MilkoScan FT 120乳品分析仪操作手册
§9．2．12 硅胶干燥盒………………………………………………………………. 70 第10章 故障查找 ................................................................................................................................ 71 §10．1 仪器故障 .............................................................................................................................. 71 §10．1．1 热保险 ....................................................................................................................... 71 §10．1．2 断电时清洗................................................................................................................ 71 §10．1．3 PC机中断时清洗 ....................................................................................................... 71 §10．1．4 清洗严重堵塞............................................................................................................ 71 §10．1．5 排除空气 ................................................................................................................... 72 §10．1．6 较低重复性的恢复 .................................................................................................... 73 §10．1．7 低清洗效率的恢复 .................................................................................................... 73 §10．2 错误信息 .............................................................................................................................. 74 第11章 化学试剂 ................................................................................................................................ 76 §11．1 清洗剂 .................................................................................................................................. 76 §11．1．1 清洗液 ........................................................................................................................ 76 §11．1．2 普通清洗剂 ................................................................................................................ 76 §11．2 调零液 .................................................................................................................................. 76 §11．3 样品准备 .............................................................................................................................. 76 §11．3．1 样品添加物 ................................................................................................................ 76 §11．3．2 稳定性监控样品 ........................................................................................................ 77 §11．3．3 重复性检测样品 ........................................................................................................ 77 §11．3．4 定标样品 .................................................................................................................... 77 §11．3．5 线性校正样品 ............................................................................................................ 77 §11．3．6 FTIR平衡液 ............................................................................................................ 78 附录A 安装和设置 ............................................................................................................................ 79 §A1 FT－120仪器的安装 ................................................................................................................ 79 §A．1．1 仪器的安放 ................................................................................................................. 79 §A．1．2 附件的安放 ................................................................................................................. 79 §A．1．3 运输器保护装置的移动和安放 ................................................................................. 79 §A．1．4 电压............................................................................................................................. 83 §A．1．5 电子连接 ..................................................................................................................... 84 §A．1．6 废液出口 ..................................................................................................................... 84 §A．1．7 稳定............................................................................................................................. 84 §A．1．8 PCIO板和ARC板的安装 ......................................................................................... 84 §A．2 FT－120仪器软件的安装 .................................................................................................. 85 §A．2．1 颜色选择 ..................................................................................................................... 85 §A．2．2 打印机安装 ................................................................................................................. 85 附录B 技术信息 ................................................................................................................................ 86 §B．1 技术说明 ............................................................................................................................... 86 §B．2 标准和支持 ........................................................................................... 错误！未定义书签。 §B．3 专利 ....................................................................................................... 错误！未定义书签。
福斯中国应用技术部 5 Foss China Application Team